Ponte Academic Journal Sep 2016, Volume 72, Issue 9 |
THE MECHANISM OF FINAL SIZE CONTROL OF L10-FEPT NANOCRYSTALS Author(s): Seyed Ali Sebt ,Zahra Bamshad, Mohammad Reza Abolhassani J. Ponte - Sep 2016 - Volume 72 - Issue 9 doi: 10.21506/j.ponte.2016.9.7 Abstract: During annealing and transition to fct-L10 phase, the FePt nanocrystals join together so their size increase. In addition, the size distribution becomes broad and their shape change. The final diameter of L10-FePt nanoparticles after annealing at 600oC depends on their coating method on the substrate. In our proposed method, we gradually contact a colloidal solution of 2.5 nm FePt nanoparticles to the spinning SiO2/Si substrate. The experimental results and discussion about the mechanism of size control indicate that the final diameter of nanoparticles as a function of rotation speed of the substrate, has a minimum at 760rpm. In these conditions the average diameter of FePt nanoarticles after annealing at 600oC for 1h is 11nm with 1.93nm standard deviation.
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